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J.MirandaM.RomeroF

10.1210/endo.142.5.8128 127 WeirG

weighing 4.2 g (14mmol) of Fmoc-Gly-OH, 2.2 g (16.8mmol) of HOBt and 0.2 g (1.4mmol) of DMAP, dissolving with DMF, adding 3.0ml of DIC (20mmol) in ice-water bath at 0 , activating for 5 minutes, adding the mixture into a reaction column, reacting for 2 hours, adding 35ml of acetic anhydride and 30ml of pyridine, mixing and sealing for 24 hours, washing three times with DCM, draining the Resin after methanol contraction to obtain 22.8 g of 1- (3-hydroxypropyl) -1H-imidazole bistrifluoromethylsulfonimide-Merrifield Resin, wherein the detection substitution degree is 0.27 mmol/g

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