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The slowed gastric emptying combined with altered gut motility creates unpredictable effects on colonic transit
This is very important because temperature has a significant impact on the result
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The crude product, containing some pentafluorophenol and Z-Trp-OPfp, was re-suspended in 2 L of ethyl acetate/hexane (1 : 1 v/v), stirred for 1 h, filtered, and air-dried to provide the 95% pure product (147.5 g, 260.7 mmol)
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